Information card for entry 7038667

Structure parameters

• Formula: C46.7 H77.3 Al2 N3.3 O4.7 Si4
• Calculated formula: C46.682 H77.318 Al2 N3.318 O4.682 Si4
• Title of publication: Aryl(silyl)amino group stabilized hydridosilanediols: synthesis and characterization and use for preparation of alumino(hydrido)siloxanes.
• Authors of publication: Wang, Xiaoping; Li, Jiancheng; Chen, Shimin; Liu, Weiping; Ye, Qingsong; Zhu, Hongping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 15
• Pages of publication: 6709 - 6717
• a: 15.214 ± 0.0005 Å
• b: 10.4426 ± 0.0003 Å
• c: 17.3308 ± 0.0005 Å
• α: 90°
• β: 103.941 ± 0.003°
• γ: 90°
• Cell volume: 2672.31 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.042
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.099
• Weighted residual factors for all reflections included in the refinement: 0.104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No