Information card for entry 7039157

Structure parameters

• Formula: C15 H23 As Br0.55 Cl1.45
• Calculated formula: C15 H23 As Br0.5484 Cl1.4516
• Title of publication: Insertion of (t)BuNC into thorium-phosphorus and thorium-arsenic bonds: phosphaazaallene and arsaazaallene moieties in f element chemistry.
• Authors of publication: Behrle, Andrew C.; Walensky, Justin R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 24
• Pages of publication: 10042 - 10049
• a: 8.3739 ± 0.0012 Å
• b: 9.1197 ± 0.0013 Å
• c: 11.6208 ± 0.0016 Å
• α: 75.718 ± 0.002°
• β: 71.528 ± 0.001°
• γ: 81.712 ± 0.002°
• Cell volume: 813.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0266
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0591
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No