Crystallography Open Database

Information card for entry 7039801

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Coordinates	7039801.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H13 F6 N9 O Os
Calculated formula	C22 H13 F6 N9 O Os
Title of publication	Osmium(ii) complexes for light-driven aerobic oxidation of amines to imines.
Authors of publication	Li, Yong-Hui; Liu, Xiao-Le; Yu, Zhen-Tao; Li, Zhao-Sheng; Yan, Shi-Cheng; Chen, Guang-Hui; Zou, Zhi-Gang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	31
Pages of publication	12400 - 12408
a	11.3688 ± 0.0008 Å
b	11.6384 ± 0.0008 Å
c	13.3026 ± 0.0009 Å
α	68.593 ± 0.002°
β	69.189 ± 0.002°
γ	84.135 ± 0.002°
Cell volume	1531.02 ± 0.19 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0639
Residual factor for significantly intense reflections	0.04
Weighted residual factors for significantly intense reflections	0.0825
Weighted residual factors for all reflections included in the refinement	0.0877
Goodness-of-fit parameter for all reflections included in the refinement	1.017
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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