Information card for entry 7040028

Structure parameters

• Formula: C156.5 H215 F13.5 N13.5 O53 Rh9 S4.5
• Calculated formula: C142 H159 F9 N13.5 O35.5 Rh9 S3
• Title of publication: A nonanuclear triangular macrocycle and a linear heptanuclear heterometallic complex based on a 2-substituted imidazole-4,5-dicarboxylate ligand.
• Authors of publication: Lin, Yue-Jian; Shan, Wei-Long; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 32
• Pages of publication: 12680 - 12684
• a: 16.272 ± 0.0008 Å
• b: 23.9463 ± 0.0011 Å
• c: 26.2849 ± 0.0012 Å
• α: 90.727 ± 0.002°
• β: 91.725 ± 0.002°
• γ: 107.527 ± 0.002°
• Cell volume: 9759.6 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1189
• Residual factor for significantly intense reflections: 0.0951
• Weighted residual factors for significantly intense reflections: 0.2675
• Weighted residual factors for all reflections included in the refinement: 0.2913
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No