Information card for entry 7040743

Structure parameters

• Formula: C63 H62 Ag Cl7 N6 P2 Pd2
• Calculated formula: C63 H62 Ag Cl7 N6 P2 Pd2
• Title of publication: Synthesis, structure and reactivity of Pd and Ir complexes based on new lutidine-derived NHC/phosphine mixed pincer ligands.
• Authors of publication: Sánchez, Práxedes; Hernández-Juárez, Martín; Álvarez, Eleuterio; Paneque, Margarita; Rendón, Nuria; Suárez, Andrés
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 42
• Pages of publication: 16997 - 17009
• a: 11.9582 ± 0.0004 Å
• b: 14.6903 ± 0.0005 Å
• c: 18.8464 ± 0.0006 Å
• α: 76.776 ± 0.002°
• β: 84.078 ± 0.002°
• γ: 79.62 ± 0.002°
• Cell volume: 3163.56 ± 0.18 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.1513
• Weighted residual factors for all reflections included in the refinement: 0.1596
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No