Information card for entry 7040949

Structure parameters

• Formula: C39 H29 Cl N4 O6 Os
• Calculated formula: C39 H29 Cl N4 O6 Os
• Title of publication: Different manifestations of enhanced π-acceptor ligation at every redox level of [Os(9-OP)L2](n), n = 2+, +, 0, - (9-OP(-) = 9-oxidophenalenone and L = bpy or pap).
• Authors of publication: Hazari, Arijit Singha; Paretzki, Alexa; Fiedler, Jan; Zalis, Stanislav; Kaim, Wolfgang; Lahiri, Goutam Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 45
• Pages of publication: 18241 - 18251
• a: 11.694 ± 0.003 Å
• b: 12.469 ± 0.004 Å
• c: 13.505 ± 0.004 Å
• α: 110.8 ± 0.003°
• β: 97.579 ± 0.001°
• γ: 112.346 ± 0.003°
• Cell volume: 1619.5 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0651
• Weighted residual factors for all reflections included in the refinement: 0.0668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No