Information card for entry 7041662

Structure parameters

• Common name: [Ni(phen)3]2{[Ni(en)2]V15Sb6O42(H2O)}x19H2O
• Chemical name: '[Ni(C12H8N2)3]2{[Ni(C2N2H8)2]V15Sb6O42(H2O)} x 19H2O'
• Formula: C76 H104 N16 Ni3 O62 Sb6 V15
• Calculated formula: C76 H96 N16 Ni3 O62 Sb6 V15
• Title of publication: In situ ligand exchange-mediated 0D/1D transformation of a polyoxovanadate.
• Authors of publication: Wendt, M.; Polzin, P.; van Leusen, J.; Näther, C; Kögerler, P; Bensch, W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 5
• Pages of publication: 1618 - 1623
• a: 21.2523 ± 0.0012 Å
• b: 31.159 ± 0.002 Å
• c: 18.7101 ± 0.0011 Å
• α: 90°
• β: 92.117 ± 0.007°
• γ: 90°
• Cell volume: 12381.4 ± 1.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.039
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.0947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No