Crystal structures and intense luminescence of tris(3-(2'-pyridyl)-pyrazolyl)borate Tb(3+) and Eu(3+) complexes with carboxylate co-ligands.
Authors of publication
Mikhalyova, Elena A.; Yakovenko, Anastasiya V.; Zeller, Matthias; Gavrilenko, Konstantin S.; Kiskin, Mikhail A.; Smola, Sergey S.; Dotsenko, Vladimir P.; Eremenko, Igor L.; Addison, Anthony W.; Pavlishchuk, Vitaly V.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2017
Journal volume
46
Journal issue
11
Pages of publication
3457 - 3469
a
34.66 ± 0.005 Å
b
10.1788 ± 0.0016 Å
c
19.762 ± 0.003 Å
α
90°
β
91.301 ± 0.002°
γ
90°
Cell volume
6970.2 ± 1.8 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
7
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0567
Residual factor for significantly intense reflections
0.0356
Weighted residual factors for significantly intense reflections
0.0731
Weighted residual factors for all reflections included in the refinement
0.0801
Goodness-of-fit parameter for all reflections included in the refinement
