Crystal structures and intense luminescence of tris(3-(2'-pyridyl)-pyrazolyl)borate Tb(3+) and Eu(3+) complexes with carboxylate co-ligands.
Authors of publication
Mikhalyova, Elena A.; Yakovenko, Anastasiya V.; Zeller, Matthias; Gavrilenko, Konstantin S.; Kiskin, Mikhail A.; Smola, Sergey S.; Dotsenko, Vladimir P.; Eremenko, Igor L.; Addison, Anthony W.; Pavlishchuk, Vitaly V.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2017
Journal volume
46
Journal issue
11
Pages of publication
3457 - 3469
a
10.2625 ± 0.0017 Å
b
14.111 ± 0.002 Å
c
15.447 ± 0.003 Å
α
72.703 ± 0.002°
β
78.079 ± 0.002°
γ
89.279 ± 0.002°
Cell volume
2086.9 ± 0.6 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.035
Residual factor for significantly intense reflections
0.0282
Weighted residual factors for significantly intense reflections
0.0649
Weighted residual factors for all reflections included in the refinement
0.0689
Goodness-of-fit parameter for all reflections included in the refinement
