Information card for entry 7041724

Structure parameters

• Formula: C74.5 H74.5 Co2 I N12.5 O6 U
• Calculated formula: C74.5 H74.5 Co2 I N12.5 O6 U
• Title of publication: Synthesis and SMM behaviour of trinuclear versus dinuclear 3d-5f uranyl(v)-cobalt(ii) cation-cation complexes.
• Authors of publication: Chatelain, Lucile; Tuna, Floriana; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5498 - 5502
• a: 31.576 ± 0.002 Å
• b: 19.4882 ± 0.0011 Å
• c: 27.13 ± 0.002 Å
• α: 90°
• β: 112.29 ± 0.009°
• γ: 90°
• Cell volume: 15447 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.1838
• Residual factor for significantly intense reflections: 0.0864
• Weighted residual factors for significantly intense reflections: 0.1943
• Weighted residual factors for all reflections included in the refinement: 0.2495
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No