Information card for entry 7041886

Structure parameters

• Common name: Ext_PhGe4 with CH2Cl2
• Chemical name: extended octaphenyl germa[4]pericyclyne
• Formula: C66 H40 Cl4 Ge4
• Calculated formula: C66 H40 Cl4 Ge4
• Title of publication: Extended germa[N]pericyclynes: synthesis and characterization.
• Authors of publication: Tanimoto, Hiroki; Fujiwara, Taro; Mori, Junta; Nagao, Tomohiko; Nishiyama, Yasuhiro; Morimoto, Tsumoru; Ito, Shunichiro; Tanaka, Kazuo; Chujo, Yoshiki; Kakiuchi, Kiyomi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 7
• Pages of publication: 2281 - 2288
• a: 13.7886 ± 0.0006 Å
• b: 13.7886 ± 0.0006 Å
• c: 15.0538 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2862.11 ± 0.19 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No