Information card for entry 7041925

Structure parameters

• Formula: C56 H44 Cl8 Ni P4
• Calculated formula: C56 H44 Cl8 Ni P4
• SMILES: [Ni]123([P](c4ccccc4[P]3(c3ccccc3)c3ccccc3)(c3ccccc3[P]1(c1ccccc1)c1ccccc1)c1c([P]2(c2ccccc2)c2ccccc2)cccc1)Cl.ClC(Cl)Cl.[Cl-].ClC(Cl)Cl
• Title of publication: On the coordination non-innocence of antimony in nickel(ii) complexes of the tetradentate (o-(Ph2P)C6H4)3Sb ligand.
• Authors of publication: Jones, J. Stuart; Wade, Casey R.; Yang, Mengxi; Gabbaï, François P
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5598 - 5604
• a: 16.6557 ± 0.0013 Å
• b: 21.835 ± 0.0018 Å
• c: 33.334 ± 0.003 Å
• α: 90°
• β: 95.711 ± 0.004°
• γ: 90°
• Cell volume: 12062.6 ± 1.7 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0743
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for significantly intense reflections: 0.1344
• Weighted residual factors for all reflections included in the refinement: 0.1414
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No