Information card for entry 7042058

Structure parameters

• Formula: C57 H48 N8 O3.34 P2 W
• Calculated formula: C57 H48 N8 O3.344 P2 W
• Title of publication: 5-(2-Pyridil)-1H-tetrazole complexes with Mo(iv) and W(iv) cyanides.
• Authors of publication: Mrowiec, A.; Jurowska, A.; Hodorowicz, M.; Szklarzewicz, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 12
• Pages of publication: 4030 - 4037
• a: 13.365 ± 0.005 Å
• b: 13.484 ± 0.005 Å
• c: 16.718 ± 0.005 Å
• α: 70.768 ± 0.005°
• β: 88.204 ± 0.005°
• γ: 63.024 ± 0.005°
• Cell volume: 2510.1 ± 1.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 125 ± 3 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0828
• Goodness-of-fit parameter for all reflections included in the refinement: 1.198
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No