Information card for entry 7042076

Structure parameters

• Common name: 16180_Complex-1-Cl
• Formula: C42 H63 Al Cl N4 P3 Rh
• Calculated formula: C42 H63 Al Cl N4 P3 Rh
• Title of publication: Structure and dynamic NMR behavior of rhodium complexes supported by Lewis acidic group 13 metallatranes.
• Authors of publication: Moore, James T.; Smith, Nicholas E.; Lu, Connie C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5689 - 5701
• a: 12.3569 ± 0.0019 Å
• b: 13.627 ± 0.002 Å
• c: 14.305 ± 0.002 Å
• α: 66.376 ± 0.002°
• β: 81.629 ± 0.002°
• γ: 75.031 ± 0.002°
• Cell volume: 2129.6 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0293
• Residual factor for significantly intense reflections: 0.0254
• Weighted residual factors for significantly intense reflections: 0.0645
• Weighted residual factors for all reflections included in the refinement: 0.0671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No