Information card for entry 7042163

Structure parameters

• Formula: C13 H29 N O2 Si
• Calculated formula: C13 H29 N O2 Si
• SMILES: [Si](OC(=O)N)(C(C)(C)C)(C(C)(C)C)C(C)(C)C
• Title of publication: Reaction of the thermo-labile triazenide Na[tBu3SiNNNSiMe3] with CO2: Formation of the imido carbonate (tBu3SiO)(Me3SiO)C=N-SitBu3 and carbamine acid (tBu3SiO)CONH2
• Authors of publication: Lerner, Hans-Wolfram; Bolte, Michael; Wagner, Matthias
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.0114 ± 0.0005 Å
• b: 13.1118 ± 0.0008 Å
• c: 14.1657 ± 0.0009 Å
• α: 77.395 ± 0.001°
• β: 89.923 ± 0.001°
• γ: 82.143 ± 0.001°
• Cell volume: 1617.38 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0718
• Weighted residual factors for significantly intense reflections: 0.1356
• Weighted residual factors for all reflections included in the refinement: 0.1511
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No