Information card for entry 7042241

Structure parameters

• Formula: C24 H35 B N8 O Pd
• Calculated formula: C24 H35 B N8 O Pd
• SMILES: [Pd]12([n]3n(c(cc3C)C)[BH](n3[n]1c(cc3C)C)n1[n]2c(C)cc1C)(/N=N/c1ccc(OC)cc1)(C)C
• Title of publication: The first palladium(iv) aryldiazenido complex: relevance for C-C coupling.
• Authors of publication: Daryanavard, Marzieh; Armstrong, David; Lough, Alan J.; Fekl, Ulrich
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 12
• Pages of publication: 4004 - 4008
• a: 7.9636 ± 0.0007 Å
• b: 12.4983 ± 0.0012 Å
• c: 13.5112 ± 0.0012 Å
• α: 89.71 ± 0.002°
• β: 87.268 ± 0.002°
• γ: 81.87 ± 0.002°
• Cell volume: 1329.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.079
• Weighted residual factors for all reflections included in the refinement: 0.0862
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No