Information card for entry 7043066

Structure parameters

• Formula: C42.5 H48 N2 O5 W
• Calculated formula: C42.5 H48 N2 O5 W
• Title of publication: Normal-to-Abnormal Rearrangement of an N-Heterocyclic Carbene with a Silylene Transition Metal Complex
• Authors of publication: Ghadwal, Rajendra S.; Rottschaefer, Dennis; Andrada, Diego Marcelo; Frenking, G.; Schürmann, Christian J.; Stammler, Georg
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 12.193 ± 0.002 Å
• b: 13.362 ± 0.002 Å
• c: 14.396 ± 0.003 Å
• α: 105.95 ± 0.02°
• β: 105.03 ± 0.02°
• γ: 110.55 ± 0.02°
• Cell volume: 1939.8 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.024
• Residual factor for significantly intense reflections: 0.0211
• Weighted residual factors for significantly intense reflections: 0.0486
• Weighted residual factors for all reflections included in the refinement: 0.0494
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No