Information card for entry 7043279

Structure parameters

• Formula: C69.6 H60.5 Co2 N12 O48.25 Sb8 V14
• Calculated formula: C69.6 H48 Co2 N12 O49.25 Sb7.88 V14
• Title of publication: An unprecedented antimonato-polyoxovanadate (SbPOVs) based on both α-[V14Sb8O42]4- and β-[V14Sb8O42]4- isomers
• Authors of publication: Cui, Xiaobing; guo, haiyang; Zhang, Xiao; xiao, lina
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 19.81131 ± 0.00015 Å
• b: 19.81131 ± 0.00015 Å
• c: 56.5195 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 22183.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0839
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for significantly intense reflections: 0.1454
• Weighted residual factors for all reflections included in the refinement: 0.1712
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No