Crystallography Open Database

Information card for entry 7043293

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Coordinates	7043293.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H35 Cl3 N P2 Re
Calculated formula	C31 H35 Cl3 N P2 Re
Title of publication	Synthesis and Characterization of Rhenium(III) Complexes with (Ph2PCH2CH2)2NR Diphosphinoamine Ligands
Authors of publication	Salvarese, Nicola; Refosco, Fiorenzo; Seraglia, Roberta; Roverso, Marco; Dolmella, Alessandro; Bolzati, Cristina
Journal of publication	Dalton Trans.
Year of publication	2017
a	11.44174 ± 0.00012 Å
b	14.86579 ± 0.00011 Å
c	19.31565 ± 0.00018 Å
α	90°
β	98.9519 ± 0.0009°
γ	90°
Cell volume	3245.39 ± 0.05 Å³
Cell temperature	297.4 K
Ambient diffraction temperature	297.4 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0305
Residual factor for significantly intense reflections	0.0225
Weighted residual factors for significantly intense reflections	0.0516
Weighted residual factors for all reflections included in the refinement	0.0536
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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