Information card for entry 7043296

Structure parameters

• Formula: C32 H38 Cl3 N2 O P2 Re
• Calculated formula: C32 H38 Cl3 N2 O P2 Re
• Title of publication: Synthesis and Characterization of Rhenium(III) Complexes with (Ph2PCH2CH2)2NR Diphosphinoamine Ligands
• Authors of publication: Salvarese, Nicola; Refosco, Fiorenzo; Seraglia, Roberta; Roverso, Marco; Dolmella, Alessandro; Bolzati, Cristina
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 12.61584 ± 0.00009 Å
• b: 14.38916 ± 0.0001 Å
• c: 18.04782 ± 0.00013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3276.24 ± 0.04 ų
• Cell temperature: 302.3 ± 0.9 K
• Ambient diffraction temperature: 302.3 ± 0.9 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.021
• Residual factor for significantly intense reflections: 0.0181
• Weighted residual factors for significantly intense reflections: 0.038
• Weighted residual factors for all reflections included in the refinement: 0.0392
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No