Information card for entry 7043710

Structure parameters

• Formula: C90 H112 F12 N10 O27 Rh4 S4
• Calculated formula: C86 H86 F12 N10 O22 Rh4 S4
• Title of publication: Stepwise construction of discrete parallelogram- and prism-shaped organometallic architectures based on half-sandwich rhodium fragments
• Authors of publication: Jin, Guo-Xin; Gao, Wen-Xi; Lin, Yue-Jian
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 15.3538 ± 0.0017 Å
• b: 17.894 ± 0.002 Å
• c: 20.376 ± 0.002 Å
• α: 109.857 ± 0.002°
• β: 91.607 ± 0.002°
• γ: 96.139 ± 0.002°
• Cell volume: 5222.7 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1416
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for significantly intense reflections: 0.1405
• Weighted residual factors for all reflections included in the refinement: 0.1714
• Goodness-of-fit parameter for all reflections included in the refinement: 0.837
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No