Information card for entry 7043884

Structure parameters

• Formula: C23.5 H22 Cl2.15 F5.5 N4 Ni O3.75
• Calculated formula: C23.686 H22 Cl2.157 F5.529 N4 Ni O3.686
• Title of publication: Heteroleptic nickel(II)-diNHC complexes and unusual ‘reverse’ carbene-transfer to silver(I)
• Authors of publication: Huynh, Han Vinh; Koh, Christine Hui Min; Nguyen, Van Ha
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 8.649 ± 0.006 Å
• b: 10.985 ± 0.008 Å
• c: 15.733 ± 0.012 Å
• α: 81.77 ± 0.016°
• β: 85.099 ± 0.018°
• γ: 70.204 ± 0.014°
• Cell volume: 1390.9 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.103
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.1518
• Weighted residual factors for all reflections included in the refinement: 0.1728
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No