Information card for entry 7044012

Structure parameters

• Common name: 3Pd(aa)2*2Pb(hfa)2
• Chemical name: tris-(palladium acetylacetonate)bis-(lead hexafluoroacetylacetonate)
• Formula: C12.5 H11.5 F6 O5 Pb0.5 Pd0.75
• Calculated formula: C12.5 H11.5 F6 O5 Pb0.5 Pd0.75
• Title of publication: Volatile heterometallics: structural diversity of palladium-lead β-diketonates and correlation with thermal properties
• Authors of publication: Krisyuk, Vladislav; Baidina, Iraida; Kryuchkova, Natalia; Logvinenko, Vladimir A.; Plyusnin, Pavel; Korolkov, Ilya V.; Zharkova, G. I.; Turgambaeva, Asiya; Igumenov, Igor K.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.874 ± 0.0003 Å
• b: 13.2443 ± 0.0004 Å
• c: 14.6006 ± 0.0004 Å
• α: 74.679 ± 0.002°
• β: 72.764 ± 0.001°
• γ: 69.446 ± 0.001°
• Cell volume: 1679.93 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0234
• Residual factor for significantly intense reflections: 0.0207
• Weighted residual factors for significantly intense reflections: 0.0494
• Weighted residual factors for all reflections included in the refinement: 0.0504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No