Information card for entry 7044202

Structure parameters

• Formula: C38.5 H30 F6 N3 O5.75 P2 Tc
• Calculated formula: C38.5 H30 F6 N3 O5.75 P2 Tc
• Title of publication: [TcII(NO)(trifluoroacetate)4F]2- - Synthesis and Reactions
• Authors of publication: Balasekaran, Samundeeswari Mariappan; Hagenbach, Adelheid; Drees, Markus; Abram, Ulrich
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 24.863 ± 0.002 Å
• b: 10.69 ± 0.001 Å
• c: 29.057 ± 0.002 Å
• α: 90°
• β: 98.96°
• γ: 90°
• Cell volume: 7628.7 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0727
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1039
• Weighted residual factors for all reflections included in the refinement: 0.1125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No