Information card for entry 7044256

Structure parameters

• Formula: C25 H54 B10 Br2 N4 Ni P2
• Calculated formula: C25 H54 B10 Br2 N4 Ni P2
• Title of publication: Bis(silylenyl)-substituted ferrocene-stabilized 6-arene iron(0) complexes: synthesis, structure and catalytic application
• Authors of publication: Driess, Matthias; Luecke, Marcel Philip; Porwal, Digvijay; Kostenko, Arseni; Zhou, Yupeng; Yao, Shenglai; Keck, Matthias; Limberg, Christian; Oestreich, Martin
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 10.1791 ± 0.0002 Å
• b: 32.1548 ± 0.0008 Å
• c: 11.359 ± 0.0002 Å
• α: 90°
• β: 92.685 ± 0.002°
• γ: 90°
• Cell volume: 3713.8 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.075
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1067
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No