Information card for entry 7044480

Structure parameters

• Formula: C17 H31 B9 Ni Ru
• Calculated formula: C17 H31 B9 Ni Ru
• Title of publication: Synthesis of 13-vertex Dimetallacarboranes by Electrophilic Insertion into 12-vertex Ruthenacarboranes
• Authors of publication: Perekalin, Dmitry S.; Lyssenko, Konstantin A.; Kudinov, Alexander R.; Corsini, Maddalena; Fabrizi de Biani, Fabrizia
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 14.285 ± 0.004 Å
• b: 10.242 ± 0.003 Å
• c: 28.482 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4167 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No