Information card for entry 7044554

Structure parameters

• Formula: C23 H46 B Cl F4 N P2 Rh
• Calculated formula: C23 H46 B Cl F4 N P2 Rh
• Title of publication: Half-Sandwich Complexes of Ir(III), Rh(III) and Ru(II) with the MaxPhos Ligand: Metal Centred Chirality and Cyclometallation
• Authors of publication: Téllez, Juan; Gallen, Albert; Ferrer, Joaquina; Lahoz, Fernando J.; García-Orduña, Pilar; Riera, Antoni; Verdaguer, Xavier; Carmona, Daniel; Grabulosa, Arnald
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.7378 ± 0.0004 Å
• b: 16.4348 ± 0.0007 Å
• c: 18.137 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2902.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0285
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0658
• Weighted residual factors for all reflections included in the refinement: 0.0672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No