Information card for entry 7044646

Structure parameters

• Formula: C73 H68 Cl6 Fe O Os P3
• Calculated formula: C73 H68 Cl6 Fe O Os P3
• Title of publication: Syntheses, structural characterisation and electronic structures of ferrocenyl-osmafuran heterobinuclear organometallic complexes
• Authors of publication: Liu, Bin; Guo, Chun-Lan; Liu, Wen-Xia; Guo, Ming-E.; Yan, Feng; Xue, Lu-Sha; Wang, Huijuan; Liu, Chang-Lin; Jin, Shan
• Journal of publication: Dalton Transactions
• Year of publication: 2017
• a: 14.7133 ± 0.001 Å
• b: 20.3718 ± 0.0013 Å
• c: 23.0817 ± 0.0015 Å
• α: 90°
• β: 103.262 ± 0.001°
• γ: 90°
• Cell volume: 6733.9 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.1132
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No