Information card for entry 7044648

Structure parameters

• Formula: C61.5 H58 Cl7 Fe O Os P3
• Calculated formula: C61.5 H58 Cl7 Fe O Os P3
• Title of publication: Syntheses, structural characterisation and electronic structures of ferrocenyl-osmafuran heterobinuclear organometallic complexes
• Authors of publication: Liu, Bin; Guo, Chun-Lan; Liu, Wen-Xia; Guo, Ming-E.; Yan, Feng; Xue, Lu-Sha; Wang, Huijuan; Liu, Chang-Lin; Jin, Shan
• Journal of publication: Dalton Transactions
• Year of publication: 2017
• a: 12.8226 ± 0.0008 Å
• b: 21.1839 ± 0.0014 Å
• c: 22.4869 ± 0.0015 Å
• α: 90°
• β: 103.809 ± 0.001°
• γ: 90°
• Cell volume: 5931.6 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.051
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.1012
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No