Information card for entry 7044993

Structure parameters

• Common name: [K(crypt-222)][(Eind)GeBr2]
• Chemical name: Eind-germylenoid
• Formula: C46 H81 Br2 Ge K N2 O6
• Calculated formula: C46 H81 Br2 Ge K N2 O6
• Title of publication: 1,2-Dihalodigermenes bearing bulky Eind groups: synthesis, characterization, and conversion to halogermylenoids.
• Authors of publication: Hayakawa, Naoki; Sugahara, Tomohiro; Numata, Yasuyuki; Kawaai, Hotaka; Yamatani, Kenta; Nishimura, Shogo; Goda, Shun; Suzuki, Yuko; Tanikawa, Tomoharu; Nakai, Hidetaka; Hashizume, Daisuke; Sasamori, Takahiro; Tokitoh, Norihiro; Matsuo, Tsukasa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 3
• Pages of publication: 814 - 822
• a: 11.288 ± 0.0009 Å
• b: 12.8136 ± 0.0007 Å
• c: 18.9434 ± 0.0017 Å
• α: 104.562 ± 0.004°
• β: 96.164 ± 0.005°
• γ: 107.936 ± 0.005°
• Cell volume: 2471.7 ± 0.3 ų
• Cell temperature: 103 K
• Ambient diffraction temperature: 103 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1184
• Weighted residual factors for all reflections included in the refinement: 0.1323
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No