Information card for entry 7045049

Structure parameters

• Formula: C64 H54 Cl6 Co N8 Sn
• Calculated formula: C64 H50 Cl6 Co N8 Sn
• Title of publication: Reaction of tin(iv) phthalocyanine dichloride with decamethylmetallocenes (M = Cr^II and Co^II). Strong magnetic coupling of spins in (Cp*₂Co⁺){Sn^IVCl₂(Pc˙^3-)}˙^-·2C₆H₄Cl₂.
• Authors of publication: Konarev, Dmitri V.; Troyanov, Sergey I.; Shestakov, Alexander F.; Yudanova, Evgeniya I.; Otsuka, Akihiro; Yamochi, Hideki; Kitagawa, Hiroshi; Lyubovskaya, Rimma N.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 4
• Pages of publication: 1243 - 1250
• a: 10.676 ± 0.001 Å
• b: 28.916 ± 0.003 Å
• c: 18.615 ± 0.002 Å
• α: 90°
• β: 98.234 ± 0.01°
• γ: 90°
• Cell volume: 5687.3 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0529
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.1156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.84344 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No