Information card for entry 7045372

Structure parameters

• Formula: C150 H157 F12 N19 O14 Rh4 S4
• Calculated formula: C140 H142 F12 N14 O14 Rh4 S4
• Title of publication: Light-initiated reversible conversion of macrocyclic endoperoxides derived from half-sandwich rhodium-based metallarectangles.
• Authors of publication: Shan, Wei-Long; Gao, Wen-Xi; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 8
• Pages of publication: 2769 - 2777
• a: 13.342 ± 0.0015 Å
• b: 22.628 ± 0.003 Å
• c: 25.834 ± 0.003 Å
• α: 95.573 ± 0.002°
• β: 90.823 ± 0.002°
• γ: 104.286 ± 0.002°
• Cell volume: 7516.5 ± 1.6 ų
• Cell temperature: 202 ± 2 K
• Ambient diffraction temperature: 202 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1572
• Residual factor for significantly intense reflections: 0.0971
• Weighted residual factors for significantly intense reflections: 0.2623
• Weighted residual factors for all reflections included in the refinement: 0.3192
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No