Information card for entry 7045508

Structure parameters

• Formula: C32 H90 Ge9 Si12
• Calculated formula: C32 H90 Ge9 Si12
• Title of publication: Synthesis of low-oxidation-state germanium clusters comprising a functional anchor group - synthesis and characterization of [(Ge⁰)₅(Ge-R)₃(Ge-(CH₂)_n-CH[double bond, length as m-dash]CH₂)] with R = Si(SiMe₃)₃.
• Authors of publication: Frischhut, Sabine; Fässler, Thomas F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 10
• Pages of publication: 3223 - 3226
• a: 16.0667 ± 0.0007 Å
• b: 17.5351 ± 0.0008 Å
• c: 23.8145 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6709.3 ± 0.5 ų
• Cell temperature: 151 ± 2 K
• Ambient diffraction temperature: 151 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0203
• Residual factor for significantly intense reflections: 0.0174
• Weighted residual factors for significantly intense reflections: 0.042
• Weighted residual factors for all reflections included in the refinement: 0.0441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No