Crystallography Open Database

Information card for entry 7045554

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Coordinates	7045554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H66 N3 O Si2 Yb
Calculated formula	C37 H66 N3 O Si2 Yb
Title of publication	Versatile reactivities of rare-earth metal dialkyl complexes supported by a neutral pyrrolyl-functionalized β-diketiminato ligand.
Authors of publication	Zhu, Xiancui; Li, Yang; Guo, Dianjun; Wang, Shaowu; Wei, Yun; Zhou, Shuangliu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	11
Pages of publication	3947 - 3957
a	23.2648 ± 0.0019 Å
b	19.3033 ± 0.0016 Å
c	21.06 ± 0.0018 Å
α	90°
β	116.292 ± 0.001°
γ	90°
Cell volume	8479.4 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293.15 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0556
Residual factor for significantly intense reflections	0.0306
Weighted residual factors for significantly intense reflections	0.0644
Weighted residual factors for all reflections included in the refinement	0.0773
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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