Information card for entry 7045672

Structure parameters

• Formula: C31 H52 N2 P2 Sn
• Calculated formula: C31 H52 N2 P2 Sn
• Title of publication: Synthesis and some coordination chemistry of the PSnP pincer-type stannylene Sn(NCH₂P^tBu₂)₂C₆H₄, attempts to prepare the PSiP analogue, and the effect of the E atom on the molecular structures of E(NCH₂P^tBu₂)₂C₆H₄ (E = C, Si, Ge, Sn).
• Authors of publication: Brugos, Javier; Cabeza, Javier A.; García-Álvarez, Pablo; Pérez-Carreño, Enrique; Polo, Diego
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 13
• Pages of publication: 4534 - 4544
• a: 23.5126 ± 0.0003 Å
• b: 11.8347 ± 0.0001 Å
• c: 23.8529 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6637.42 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0342
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0816
• Weighted residual factors for all reflections included in the refinement: 0.0841
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No