Metal complexes of a novel heterocyclic benzimidazole ligand formed by rearrangement-cyclization of the corresponding Schiff base. Electrosynthesis, structural characterization and antimicrobial activity.
Authors of publication
Casanova, I.; Durán, M L; Viqueira, J.; Sousa-Pedrares, A; Zani, F.; Real, J. A.; García-Vázquez, J A
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2018
Journal volume
47
Journal issue
12
Pages of publication
4325 - 4340
a
28.212 ± 0.006 Å
b
7.6096 ± 0.0017 Å
c
14.583 ± 0.003 Å
α
90°
β
106.955 ± 0.004°
γ
90°
Cell volume
2994.6 ± 1.1 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.1488
Residual factor for significantly intense reflections
0.0405
Weighted residual factors for significantly intense reflections
0.0742
Weighted residual factors for all reflections included in the refinement
0.1015
Goodness-of-fit parameter for all reflections included in the refinement
