Metal complexes of a novel heterocyclic benzimidazole ligand formed by rearrangement-cyclization of the corresponding Schiff base. Electrosynthesis, structural characterization and antimicrobial activity.
Authors of publication
Casanova, I.; Durán, M L; Viqueira, J.; Sousa-Pedrares, A; Zani, F.; Real, J. A.; García-Vázquez, J A
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2018
Journal volume
47
Journal issue
12
Pages of publication
4325 - 4340
a
13.703 ± 0.003 Å
b
9.786 ± 0.002 Å
c
20.08 ± 0.004 Å
α
90°
β
107.637 ± 0.004°
γ
90°
Cell volume
2566.1 ± 0.9 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0809
Residual factor for significantly intense reflections
0.0372
Weighted residual factors for significantly intense reflections
0.0858
Weighted residual factors for all reflections included in the refinement
0.1014
Goodness-of-fit parameter for all reflections included in the refinement