Synthesis, structure and magnetic properties of tris(pyrazolyl)methane lanthanide complexes: effect of the anion on the slow relaxation of magnetization.
Authors of publication
Long, Jérôme; Lyubov, Dimitry M.; Mahrova, Tatyana V.; Cherkasov, Anton V.; Fukin, Georgy K.; Guari, Yannick; Larionova, Joulia; Trifonov, Alexander A.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2018
Journal volume
47
Journal issue
15
Pages of publication
5153 - 5156
a
10.8169 ± 0.0003 Å
b
14.8226 ± 0.0005 Å
c
16.2864 ± 0.0005 Å
α
90°
β
96.0506 ± 0.0011°
γ
90°
Cell volume
2596.73 ± 0.14 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0148
Residual factor for significantly intense reflections
0.0137
Weighted residual factors for significantly intense reflections
0.0346
Weighted residual factors for all reflections included in the refinement
0.035
Goodness-of-fit parameter for all reflections included in the refinement