Information card for entry 7045788

Structure parameters

• Formula: C25 H35 N7 O3 S2 Zn
• Calculated formula: C25 H35 N7 O3 S2 Zn
• Title of publication: Four-coordinated see-saw N-(aryl)-2-(propan-2-ylidene)hydrazinecarbothioamide complexes of nickel(ii), copper(ii) and zinc(ii) and their propensity for catalytic cyclisation.
• Authors of publication: Tarai, Arup; Baruah, Jubaraj B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 14
• Pages of publication: 4921 - 4930
• a: 7.8976 ± 0.0008 Å
• b: 11.1979 ± 0.0011 Å
• c: 17.2554 ± 0.0016 Å
• α: 98.13 ± 0.008°
• β: 92.775 ± 0.008°
• γ: 91.666 ± 0.008°
• Cell volume: 1507.9 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1739
• Residual factor for significantly intense reflections: 0.0687
• Weighted residual factors for significantly intense reflections: 0.0814
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No