Information card for entry 7046171

Structure parameters

• Formula: C13 H29 N3 Si2 Sn
• Calculated formula: C13 H29 N3 Si2 Sn
• Title of publication: Synthesis, characterisation and thermal properties of Sn(ii) pyrrolide complexes.
• Authors of publication: Parish, James D.; Snook, Michael W.; Johnson, Andrew L.; Kociok-Köhn, Gabriele
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 23
• Pages of publication: 7721 - 7729
• a: 11.8512 ± 0.0004 Å
• b: 10.4036 ± 0.0003 Å
• c: 15.6557 ± 0.0005 Å
• α: 90°
• β: 96.431 ± 0.003°
• γ: 90°
• Cell volume: 1918.13 ± 0.11 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0596
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No