Information card for entry 7046269

Structure parameters

• Formula: C38 H30 N2 Ni O2 P2
• Calculated formula: C38 H30 N2 Ni O2 P2
• Title of publication: Ni(ii) complexes of the phosphine-oxime Ph₂PC₆H₄-2-CH[double bond, length as m-dash]NOH.
• Authors of publication: Basu, Debashis; Woods, Toby J.; Rauchfuss, Thomas B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 21
• Pages of publication: 7256 - 7262
• a: 23.4743 ± 0.0008 Å
• b: 13.0781 ± 0.0004 Å
• c: 20.2265 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6209.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0287
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections included in the refinement: 0.0627
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No