Information card for entry 7046297

Structure parameters

• Formula: C91 H131 Rh4 Si4 Sn2
• Calculated formula: C91 H131 Rh4 Si4 Sn2
• Title of publication: Heterobimetallic triple-decker complexes derived from a dianionic aromatic stannole ligand.
• Authors of publication: Saito, Masaichi; Matsunaga, Naoki; Hamada, Jumpei; Furukawa, Shunsuke; Minoura, Mao; Wegner, Susann; Barthel, Juri; Janiak, Christoph
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 27
• Pages of publication: 8892 - 8896
• a: 11.32 ± 0.0008 Å
• b: 19.1507 ± 0.0013 Å
• c: 21.3105 ± 0.0015 Å
• α: 103.801 ± 0.001°
• β: 93.304 ± 0.001°
• γ: 106.755 ± 0.001°
• Cell volume: 4256.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.021
• Residual factor for significantly intense reflections: 0.019
• Weighted residual factors for significantly intense reflections: 0.0464
• Weighted residual factors for all reflections included in the refinement: 0.0478
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No