Information card for entry 7046306

Structure parameters

• Formula: C27 H43 N2 P
• Calculated formula: C27 H43 N2 P
• Title of publication: Reactivity studies of an imine-functionalised phosphaalkene; unusual electrostatic and supramolecular stabilisation of a σ²λ³-phosphorus motif via hydrogen bonding.
• Authors of publication: Morales Salazar, Daniel; Gupta, Arvind Kumar; Orthaber, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 31
• Pages of publication: 10404 - 10409
• a: 14.8002 ± 0.0011 Å
• b: 10.1736 ± 0.0008 Å
• c: 17.7991 ± 0.0014 Å
• α: 90°
• β: 106.389 ± 0.001°
• γ: 90°
• Cell volume: 2571.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0601
• Weighted residual factors for significantly intense reflections: 0.1644
• Weighted residual factors for all reflections included in the refinement: 0.1786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No