Information card for entry 7046360

Structure parameters

• Formula: C41 H53 Mg N5 Si
• Calculated formula: C41 H53 Mg N5 Si
• Title of publication: 1,4-Dihydropyridyl complexes of magnesium: synthesis by pyridine insertion into the magnesium-silicon bond of triphenylsilyls and catalytic pyridine hydrofunctionalization.
• Authors of publication: Lemmerz, L. E.; Spaniol, T. P.; Okuda, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12553 - 12561
• a: 7.5892 ± 0.0008 Å
• b: 14.8942 ± 0.0017 Å
• c: 18.236 ± 0.002 Å
• α: 67.9347 ± 0.0019°
• β: 81.964 ± 0.002°
• γ: 78.815 ± 0.002°
• Cell volume: 1869 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1487
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No