Information card for entry 7046375

Structure parameters

• Formula: C16 H48 Mo12 N4 Na5 O74 Sb5
• Calculated formula: C16 H48 Mo12 N4 Na5 O74 Sb5
• Title of publication: Synthesis and characterization of a Sb(v)-containing polyoxomolybdate serving as a catalyst for sulfoxidation.
• Authors of publication: Lu, Jingkun; Wang, Yaping; Ma, Xinyi; Niu, Yanjun; Singh, Vikram; Ma, Pengtao; Zhang, Chao; Niu, Jingyang; Wang, Jingping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 24
• Pages of publication: 8070 - 8077
• a: 12.2579 ± 0.0007 Å
• b: 23.8635 ± 0.0014 Å
• c: 13.8297 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4045.4 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 7
• Space group number: 63
• Hermann-Mauguin space group symbol: C m c m
• Hall space group symbol: -C 2c 2
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.1359
• Weighted residual factors for all reflections included in the refinement: 0.1437
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No