Information card for entry 7046435

Structure parameters

• Common name: [(AmidA-H2)3Np][ClO4](H2O)2
• Formula: C15 H32 Cl N9 Np O14
• Calculated formula: C15 H32 Cl N9 Np O14
• Title of publication: Complexation-assisted reduction: complexes of glutaroimide-dioxime with tetravalent actinides (Np(iv) and Th(iv)).
• Authors of publication: Zhang, Zhicheng; Parker, Bernard F.; Lohrey, Trevor D.; Teat, Simon J.; Arnold, John; Rao, Linfeng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 24
• Pages of publication: 8134 - 8141
• a: 25.76 ± 0.02 Å
• b: 10.221 ± 0.007 Å
• c: 11.28 ± 0.008 Å
• α: 90°
• β: 108.573 ± 0.006°
• γ: 90°
• Cell volume: 2815 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0198
• Residual factor for significantly intense reflections: 0.0193
• Weighted residual factors for significantly intense reflections: 0.0543
• Weighted residual factors for all reflections included in the refinement: 0.055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No