Information card for entry 7046493

Structure parameters

• Formula: C76 H62 N4 P2
• Calculated formula: C76 H62 N4 P2
• Title of publication: New synthetic strategies leading to [RNPNR]^- anions and the isolation of the [P(Nt-Bu)₃]^3- trianion.
• Authors of publication: Vrána, Jan; Jambor, Roman; R°uŽička, Aleš; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 25
• Pages of publication: 8434 - 8441
• a: 13.406 ± 0.004 Å
• b: 29.17 ± 0.009 Å
• c: 14.794 ± 0.004 Å
• α: 90°
• β: 94.859 ± 0.011°
• γ: 90°
• Cell volume: 5764 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.1041
• Weighted residual factors for all reflections included in the refinement: 0.1082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No