Crystallography Open Database

Information card for entry 7046495

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Coordinates	7046495.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C11 H29 Li N3 P
Calculated formula	C11 H31 Li N3 P
Title of publication	New synthetic strategies leading to [RNPNR]<sup>-</sup> anions and the isolation of the [P(Nt-Bu)<sub>3</sub>]<sup>3-</sup> trianion.
Authors of publication	Vrána, Jan; Jambor, Roman; RůŽička, Aleš; Dostál, Libor
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	25
Pages of publication	8434 - 8441
a	9.662 ± 0.0007 Å
b	16.212 ± 0.0016 Å
c	9.875 ± 0.0004 Å
α	90 ± 0.007°
β	104.96 ± 0.006°
γ	90 ± 0.006°
Cell volume	1494.4 ± 0.2 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0529
Residual factor for significantly intense reflections	0.0412
Weighted residual factors for significantly intense reflections	0.1084
Weighted residual factors for all reflections included in the refinement	0.1215
Goodness-of-fit parameter for all reflections included in the refinement	1.091
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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