Information card for entry 7046525

Structure parameters

• Formula: C5 H11 K O
• Calculated formula: C5 H11 K O
• Title of publication: The hetero-cubane structures of the heavy alkali metal tert-amyloxides [MOCMe₂Et]₄ (M = K, Rb, Cs).
• Authors of publication: Kaiser, Maximillian; Klett, Jan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12582 - 12586
• a: 8.2509 ± 0.0004 Å
• b: 8.2509 ± 0.0004 Å
• c: 20.346 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1385.1 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0228
• Residual factor for significantly intense reflections: 0.0222
• Weighted residual factors for significantly intense reflections: 0.0568
• Weighted residual factors for all reflections included in the refinement: 0.0571
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No