Information card for entry 7046548

Structure parameters

• Formula: C36 H58 O P Si U
• Calculated formula: C36 H58 O P Si U
• Title of publication: Four-electron reduction chemistry using a uranium(iii) phosphido complex.
• Authors of publication: Rungthanaphatsophon, Pokpong; Barnes, Charles L.; Kelley, Steven P.; Walensky, Justin R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 25
• Pages of publication: 8189 - 8192
• a: 9.6794 ± 0.0005 Å
• b: 20.3019 ± 0.0012 Å
• c: 18.3009 ± 0.0011 Å
• α: 90°
• β: 97.346 ± 0.002°
• γ: 90°
• Cell volume: 3566.8 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0465
• Weighted residual factors for all reflections included in the refinement: 0.0505
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No